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Yayın Preliminary TL and OSL investigations of obsidian samples(Univ Agean, Dept Mediterranean Stud, 2010) Polymeris, George S.; Gogou, D.; Afouxenidis, Dimitrios; Rapti, Sofia; Tsirliganis, Nestor C.; Kitis, GeorgeObsidian is a volcaniclastic mineral extremely hard to break, which was used in prehistoric Greece (and elsewhere in the World), in order to provide tools, weapons, knives and arrowheads. The present work aims to characterize this extremely precious tool stone by using both thermoluminescence (TL) and optically stimulated luminescence (OSL) techniques and investigate its potential use for luminescence dating purposes. Basic TL and OSL properties, such as TL and OSL thermal and optical stability, repeatability, TL and LM-OSL glow curve shape and mainly the linearity of the TL and OSL signals as a function of beta dose were investigated. Artificially irradiated samples indicate all promising luminescence features, such as the 110 degrees C TL peak and dose response sub-linearity for intermediate doses, quick and effective bleaching all over the entire TL glow curve, along with quite linear CW-OSL dose response for doses larger than 5 Gy. The lack of predose sensitisation indicates the suitability of the material for single aliquot measurements. Furthermore, several features provide indications that the signal does not relate to quartz, but in fact to other silicates. Unfortunately, both lack of bleaching ability for NIL signal, along with a peculiar shape of NOSL, provide major difficulties in dating applications.Yayın Relative response of TL and component-resolved OSL to alpha and beta radiations in annealed sedimentary quartz(Pergamon-Elsevier Science Ltd, 2011-10) Polymeris, George S.; Afouxenidis, Dimitrios; Raptis, Spyridoula; Liritzis, Ioannis; Tsirliganis, Nestor C.; Kitis, GeorgeKnowledge of the relative luminescence response to alpha and beta radiation is very important in TL and OSL dating. In the present study the relative alpha to beta response is studied in a sedimentary quartz sample, previously fired at 900 degrees C for 1 h, in the dose region between 1 and 128 Gy, for both thermoluminescence (T) and linearly modulated optically stimulated luminescence (LM - OSL). The LM OSL measurements were performed at room temperature and at 125 degrees C. All OSL signals were deconvolved into their individual components. Comparison of OSL curves after alpha and beta irradiation strongly supports that quartz OSL components follow first order kinetics in both cases. In the case of TL, the relative alpha to beta response is found to be very different for each TL glow-peak, but it does not depend strongly on irradiation dose. In the case of LM OSL measurements, it is found that the relative behaviour of the alpha to beta response is different for three distinct regions, namely the fast OSL component, the region of medium OSL component originating from the TL glow-peak at 110 degrees C when stimulation takes place at room temperature and finally the region of slow OSL component. Following stimulation at ambient temperature, the relative alpha to beta response of all components was not observed to depend significantly on dose, with the value of ratio being 0.03 and a tendency to decrease with increasing dose. However, in the case of measurements performed at 125 degrees C, the relative response of the fast components is much enhanced, and for the remaining components it increases with increasing dose. Special care must be taken to examine the relative alpha to beta response of the fast component at 125 degrees C which contrasts the relative response of the TL peak at ca. 325 degrees C. The implications for the dating of annealed quartz are also briefly discussed.Yayın Thermal quenching of thermoluminescence in quartz samples of various origin(Elsevier Science BV, 2011-03-15) Subedi, Bhagawan; Oniya, Ebenezer O.; Polymeris, George S.; Afouxenidis, Dimitrios; Tsirliganis, Nestor C.; Kitis, GeorgeThe effect of thermal quenching stands among the most important properties in the thermoluminescence (TL) of quartz on which many applications of TL are based. Since the quartz samples used in various applications are all of different origin it is useful to investigate whether the values of the thermal quenching parameters, i.e. the activation energy for thermal quenching W and a parameter C which describes the ratio of non-radiative to radiative luminescence transitions, evaluated mainly in specific quartz samples can be extrapolated to quartz samples of unknown origin as well as to quartz samples which are annealed at high temperatures. In the present work the TL glow curve of a series of un-annealed and annealed natural and synthetic quartz samples were studied as a function of the heating rate between 0.25 K/s and 16 K/s. Using an indirect fitting method it was found that the thermal quenching parameters W and C in most of the quartz samples are very similar to the values accepted in the literature. Furthermore, in some cases the thermal quenching parameters Wand Care not the same for all TL glow-peaks in the same glow-curve. Finally, the strong external treatment of annealing the quartz samples at very high temperature can also influence at least one of the thermal quenching parameters.Yayın Thermal quenching of thermoluminescence in quartz samples of various origins(Univ Agean, Dept Mediterranean Stud, 2010) Subedi, Bhagawan; Afouxenidis, Dimitrios; Polymeris, George S.; Bakoglidis, Konstantinos D.; Raptis, Spyridoula; Tsirliganis, Nestor C.; Kitis, GeorgeThe effect of thermal quenching plays an important role in the thermoluminescence (TL) of quartz on which many applications of TL are based. In present work it is investigated that the thermal quenching parameters i.e. the activation energy W and the dimensionless parameter C, are more or less the same for every kind of quartzes or sample dependent on strong external treatment like a high temperature annealing. This preliminary investigation of seven quartz samples of different origin showed that the thermal quenching parameters W and C are common (universal) for most of the quartz samples.Yayın Thermally assisted OSL from deep traps in Al2O3:C(Pergamon-Elsevier Science Ltd, 2010-03) Polymeris, George S.; Raptis, Spyridoula; Afouxenidis, Dimitrios; Tsirliganis, Nestor C.; Kitis, GeorgeThe present work suggests an alternative experimental method in order to not only measure the signal of the deep traps in Al2O3:C without heating the sample to temperatures greater than 500 degrees C, but also use this signal for high dose level dosimetry purposes as well. This method consists of photo transfer OSL measurements performed at elevated temperatures using the blue LEDs (470 nm, FWHM 20 nm) housed at commercial Riso TL/OSL systems, after the sample was previously heated up to 500 degrees C in order to empty its main TL dosimetric trap. The influence of this procedure on specific features such as glow curve shape and sensitivity of the main TL glow peak was also studied.Yayın TL and OSL response of turquoise for dosimetric application(University of Aegean, 2010) Subedi, Bhagawan; Afouxenidis, Dimitrios; Polymeris, George S.; Tsirliganis, Nestor C.; Paraskevopoulos, Konstantinos M.; Kitis, GeorgeTurquoise is one of the amongst first gem stones used in jewelry and possessing cultural value since 2000 BC (at least). This work attempts characterize this stone scientifically using both thermally (TL) and optically stimulated luminescence (OSL) techniques. The experimental investigation included 1) the study of the natural TL and OSL signals, 2) the reproducibility of TL sensitivity over repeated irradiation and TL readout cycles, 3) dependence of sensitivity on annealing temperatures and 4) the TL and OSL dose response curves. The potential use of the TL and OSL techniques in determination of provenance, accidental dosimetry and probably to authenticity and dating purposes are then discussed.
