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Yayın The firing temperature of pottery from ancient Mesopotamia, Turkey, using luminescence methods: a case study for different grain-size fractions(Wiley-Blackwell, 2014-10) Polymeris, George S.; Güneç Kıyak, Nafiye; Koul, Dileep K.; Kitis, GeorgeThe assessment of the firing temperature of a prehistoric pottery sample collected from ancient Mesopotamia, Turkey was studied using luminescence techniques. The methods for this estimation involved the observation of the thermal and pre-dose sensitization with various re-firing temperatures for both TL and the OSL signals. In the former case, the 110 degrees C TL peak and the rest of the glow curve were used as proxies in this study. In the framework of a first attempt to investigate the impact of grain-size dependence on the sensitization of the luminescence signals, the aforementioned study was performed with four different pottery grain-size fractions: (i) less than 60m, (ii) 60-90m, (iii) 90-180m and (iv) 180-250m. The results clearly demonstrated the firing temperature mark of approximate to 500 degrees C in for the grain size of 90-180m, whileas in the case of the lower grain-size fractiona third proxy, the ratio of the pre-dosed to the thermal sensitization, was seen to indicate the firing temperature. The remaining two grain-size fractions failed to provide any meaningful results with regard to the firing temperature estimation. The dependence of the TL characteristics on the grain size was explained in the framework of the mixed mineralogy.Yayın Preliminary results towards the equivalence of transformed continuous-wave Optically Stimulated Luminescence (CW-OSL) and linearly-modulated (LM-OSL) signals in quartz(Versita, 2011-09) Kitis, George; Polymeris, George S.; Güneç Kıyak, Nafiye; Pagonis, VasilisThe present paper presents a comparative experimental study of two commonly measured Optically Stimulated Luminescence (OSL) signals in quartz. The experimental study measures both the continuous wave OSL (CW-OSL) and the linearly modulated (LM-OSL) signals from the same quartz sample for a range of stimulation temperatures between 180 and 280A degrees C, while the former is transformed to pseudo LM-OSL (ps LM-OSL). A computerized deconvolution curve analysis of the LM-OSL and ps LM-OSL signals was carried out, and the contributions of several OSL components to the initial OSL signal (0.1 s) were shown to be independent of the stimulation temperature used during the measurement. It was also found that the composite OSL (0.1 s) signal consists mainly of the first two OSL components present in the OSL curves. The equivalence of the ps LM-OSL (transformed CW-OSL) and of LM-OSL measurements was also examined by an appropriate choice of the experimental stimulation times, and of the stimulation power of the blue LEDs used during the measurement.Yayın Component resolved IR bleaching study of the blue LM-OSL signal of various quartz samples(Wind-J Wojewoda Publ Co, 2008-01-01) Polymeris, George S.; Güneç Kıyak, Nafiye; Kitis, GeorgeThe present work provides an initial component resolved analysis concerning the effect of infra-red (IR) exposure at elevated temperatures on the blue LM-OSL signal of quartz (stimulated at 470 nm). The study was performed on a total of seven quartz samples, among which five originated from Turkey, one from Greece and one synthetic quartz sample. For these quartz samples, the presence of 6 or even 7 independent LM-OSL components was previously reported, after the application of a computerized decomposition analysis. IR bleaching of each one of these components is studied and compared to the respective signal reduction due to the same thermal treatment solely. It is clearly demonstrated that IR stimulation at temperatures above 50 degrees C does not deplete only the fast component in most sedimentary quartz samples studied. Net depletion of fast and medium components resulting from IR exposure is sample-dependent and occurs faster as the stimulation temperature increases. Weak IR bleaching of slow components is also reported in some cases, being more effective for stimulation temperatures up to 100 degrees C. No depletion of either the medium or the slow components was detected for stimulation temperatures above 150 degrees C. Finally, IR does not stimulate any of the LM-OSL components in the case of the synthetic quartz sample.
