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Yayın A new late holocene eolianite record from Altinkum Beach, North Cyprus(Scientific technical research council Turkey-Tubitak, 2012-06) Erginal, Ahmet Evren; Güneç Kıyak, Nafiye; Ertek, Topçu AhmetIn this study, we investigated the main depositional characteristics and obtained Optically Stimulated Luminescence (OSL) ages of coastal eolianite on the north coast of Cyprus, where this occurrence had not previously been recorded. Based on EDX/SEM and XRD data and field observations, the studied eolianite that crops out between elevations of 1 m and 14 m a.s.l. is made up predominantly of quartz grains, most of which consist of medium- to fine-grained sand. The rock comprises aragonite, calcite and quartz with lesser amounts of bornite and hematite as accessory minerals. OSL ages indicated that the initial deposition of eolianite sands took place at 1.51 +/- 0.21 ka years ago.Yayın Investigating the thermally transferred optically stimulated luminescence source trap in fired geological quartz(Pergamon-Elsevier Science Ltd, 2014-03) Koul, Dileep K.; Patil, Pravinkumar G.; Oniya, Ebenezer O.; Polymeris, George S.The pre-dosed thermoluminescence (TL) emission of quartz has been found to be useful in retrospective dosimetry and archaeometry. Though the pre-dosed optically stimulated luminescence (OSL) and emissions have been reported to be similar, the former has been found to be un-reliable for the equivalent dose estimation. As this measurement protocol involves thermal heating at around 400 degrees C, the work reported in this paper investigated the influence of this heating on the OSL using fired specimens from various regions. The results suggested that the discrepancy in the behaviour of two emissions is caused by the presence of the thermally transferred optically stimulated luminescence (TT-OSL) induced by thermal-activation involved in the pre-dose treatment. This transferred signal was observed to be very significant in the case of samples containing a prominent higher-temperature TL peak at similar to 375 degrees C. The characterization of this signal based on (i) the nature of the glow curves, (ii) thermal-annealing of the OSL trap, (iii) observation of the TT-OSL, (iv) bleaching of the source trap and (v) the correlation between TL and OSL seems to suggest that the trap corresponding to this TL peak is the source trap in the TT-OSL emission mechanism.Yayın Component resolved OSL dose response and sensitization of various sedimentary quartz samples(Elsevier Ltd, 2007-02) Güneç Kıyak, Nafiye; Polymeris, George S.; Kitis, GeorgeThe structure of the linearly modulated optically stimulated luminescence (LM-OSL) signal was studied for four sedimentary quartz samples, collected from different sites around Istanbul, Turkey. Applying a computerized deconvolution analysis to the LM-OSL curves, at least six individual components of first-order kinetics were identified and photoionization cross-section of each component was evaluated. The OSL dose-response curve of each component for each quartz sample was obtained, showing a remarkable differentiation from component to component. The behavior of a highly dosed sample to successive LM-OSL measurements was also studied showing a stable recuperation signal in the position of the "slow" and "medium" components and high resistance to OSL bleaching of the "slow" component. The individual sensitivity of each component as a function of the activation temperature was obtained. The sensitivity of each component was normalized over the respective sensitivity of the glow-peak at 110 degrees C of quartz in order to investigate the ability of the 110 degrees C glow-peak to act as a correction factor for all components of the LM-OSL curves examined.Yayın Effect of annealing temperature on determining trap depths of quartz by various heating rates method(Pergamon-Elsevier Science, 2001-12) Güneç Kıyak, Nafiye; Buluş, E.The aim of this study is to determine the trap parameters (trap depth E, frequency factors) of quartz using various heating rates method and also to investigate the effect of annealing temperature on determining trap depths. The method is based on the positions of the thermoluminescence peaks, obtained from the change in temperature of the peak at maximum caused by changing the heating rate at which the sample is measured. In the present work, powder quartz samples were annealed first at different temperatures before irradiation. Then samples irradiated to different doses were measured with a TL reader at different heating rates and the glow curves were recorded. In order to calculate the trap depth E and the frequency factor s, the glow parameter T-m was determined experimentally from the glow curve by measuring the shift of the maximum peak temperature depending on heating rate beta. The calculation of trap parameters was repeated for each annealing temperature. Then the effect of annealing temperature on trap depths calculated by the various heating rates method was evaluated.Yayın Equivalent dose in quartz from young samples using the SAR protocol and the effect of preheat temperature(Pergamon-Elsevier Science Ltd, 2006-09) Güneç Kıyak, Nafiye; Canel, TimurMajor concerns in the dating of samples younger than a few hundred years by the optically stimulated luminescence (OSL) technique are thermal transfer and partial bleaching. Thermal transfer during preheating enhances the OSL signal due to the charge transfer from thermally sensitive, but light-insensitive, traps to optical centres of quartz and results in an overestimate in equivalent dose, especially for very young samples. In this study, the single-aliquot regenerative-dose protocol is used to obtain values of equivalent dose (D-e) from young samples taken from various environments around Istanbul. Within this framework, we aim to investigate the effect of preheat temperature on equivalent dose from 150 to 300 degrees C, the reproducibility of De measurements for young deposits and the contribution from thermal transfer of charge to the equivalent dose estimation. It was observed that the measured dose is influenced significantly by preheat temperature and the increase in the De is clearly due to thermal transfer of charge from deep thermally sensitive traps to OSL trap during preheating of the samples prior to the main OSL measurements.Yayın Reconstruction of thermally quenched glow curves in quartz(Pergamon-Elsevier Science Ltd, 2012-04) Subedi, Bhagawan; Polymeris, George S.; Tsirliganis, Nestor C.; Pagonis, Vasilis; Kitis, GeorgeThe experimentally measured thermoluminescence (TL) glow curves of quartz samples are influenced by the presence of the thermal quenching effect, which involves a variation of the luminescence efficiency as a function of temperature. The real shape of the thermally unquenched TL glow curves is completely unknown. In the present work an attempt is made to reconstruct these unquenched glow curves from the quenched experimental data, and for two different types of quartz samples. The reconstruction is based on the values of the thermal quenching parameter W (activation energy) and C (a dimensionless constant), which are known from recent experimental work on these two samples. A computerized glow-curve deconvolution (CGCD) analysis was performed twice for both the reconstructed and the experimental TL glow curves. Special attention was paid to check for consistency between the results of these two independent CGCD analyses. The investigation showed that the reconstruction attempt was successful, and it is concluded that the analysis of reconstructed TL glow curves can provide improved values of the kinetic parameters E, s for the glow peaks of quartz. This also leads to a better evaluation of the half-lives of electron trapping levels used for dosimetry and luminescence dating.Yayın Component-resolved thermal stability and recuperation study of the LM-OSL curves of four sedimentary quartz samples(Elsevier Ltd, 2007-09) Kitis, George; Polymeris, George S.; Güneç Kıyak, NafiyeThermal stability as well as recuperation stands among the crucial general characteristics of different OSL components in quartz. Through a series of thermal stability and recuperation experiments, in conjunction with curve fitting studies, a component resolved analysis is carried out, studying these two aspects for the OSL components identified ill quartz samples collected from sites around Istanbul. A thermally unstable ultra-fast component is reported, which is almost totally removed by heating up to 250-280 degrees C. Most slow and medium components show a stability temperature region between 200 and 350 degrees C, whereas the thermal stability of the final slow component is limited Lip to almost 300 degrees C. No detectable recuperation occurs for the first five components reported. The greatest recuperation occurred in the sixth component, despite the fact that it was less than 1%.Yayın Component resolved IR bleaching study of the blue LM-OSL signal of various quartz samples(Wind-J Wojewoda Publ Co, 2008-01-01) Polymeris, George S.; Güneç Kıyak, Nafiye; Kitis, GeorgeThe present work provides an initial component resolved analysis concerning the effect of infra-red (IR) exposure at elevated temperatures on the blue LM-OSL signal of quartz (stimulated at 470 nm). The study was performed on a total of seven quartz samples, among which five originated from Turkey, one from Greece and one synthetic quartz sample. For these quartz samples, the presence of 6 or even 7 independent LM-OSL components was previously reported, after the application of a computerized decomposition analysis. IR bleaching of each one of these components is studied and compared to the respective signal reduction due to the same thermal treatment solely. It is clearly demonstrated that IR stimulation at temperatures above 50 degrees C does not deplete only the fast component in most sedimentary quartz samples studied. Net depletion of fast and medium components resulting from IR exposure is sample-dependent and occurs faster as the stimulation temperature increases. Weak IR bleaching of slow components is also reported in some cases, being more effective for stimulation temperatures up to 100 degrees C. No depletion of either the medium or the slow components was detected for stimulation temperatures above 150 degrees C. Finally, IR does not stimulate any of the LM-OSL components in the case of the synthetic quartz sample.Yayın LM-OSL thermal activation curves of quartz: Relevance to the thermal activation of the 110 degrees C TL glow-peak(Pergamon-Elsevier Science Ltd, 2008-01) Güneç Kıyak, Nafiye; Polymeris, George S.; Kitis, GeorgeThe thermally activated characteristics (TAC) of the linearly modulated optically stimulated luminescence (LM-OSL) signals of seven quartz samples from different origin were studied relative to the TAC of their respective thermoluminescence (TL) glow-peaks at 110 degrees C. Within the framework of the study the TAC behavior of the LM-OSL was investigated by measuring the OSL signal at room temperature (RT) with the 110 degrees C glow-peak present during OSL measurements, as well as, at 125 degrees C without the glow-peak at 110 degrees C removed by a cut-heat at 180 degrees C prior to OSL measurement. The LM-OSL curves were analyzed into individual components using a computerized deconvolution procedure. It was found that all individual LM-OSL components of each kind of quartz follow the TAC behavior of the respective TL glow-peak at 110 degrees C. The fourth component of the LM-OSL curve, centered at about t(m) = 400 s, appeared when the OSL measurements were performed at RT, whereas it was absent when the OSL measurement were performed at 180 degrees C. It is suggested that this component is closely related with the TL glow-peak at 110 degrees C.
